一、电子烟释放物技术要求
1.气溶胶释放稳定性
|
Test Items |
Limit 限值 |
Test Method |
|
气溶胶释放稳定性 |
气溶胶捕集的每个检测结果与平均值的相对偏差不超过25% |
附录C |
电子烟抽烟机
1）气溶胶捕集量的测定条件：
电子烟吸烟机条件（抽吸时间：3±0.1s,抽吸频率：30±0.5s，抽吸容量55±0.3mL）
测试电子烟样品数量为3支（准备样品至少抽吸数量的3倍）
口数大于100口：每抽吸20口捕集到同一张滤片上，依次抽吸5次，取第1，3，5张滤片进行分析;
口数大于60口：每抽吸20口捕集到同一张滤片上，依次抽吸3次，分别对张滤片进行分析;
口数小于60口：每抽吸10口捕集到同一张滤片上，依次抽吸3次，分别对张滤片进行分析;
2.烟碱释放稳定性
|
Test Items |
Limit 限值 |
Test Method |
|
烟碱释放稳定性 |
烟碱释放量每个检测结果与平均值的相对偏差不超过25% |
附录I |
气相色谱仪
3.羰基化合物限量
|
Category |
Test Items |
Limit |
Test Method |
|
Carbonyl Compounds |
Formaldehyde |
200 |
附录J |
|
Acetaldehyde |
3200 |
||
|
Acrolein |
16 |
||
|
Diacetyl(2，3-Butadione) |
140 |
4.重金属限量
|
Category |
Test Items |
Limit |
Test Method |
|
Heavy Metals |
Cd(Cadmium)镉 |
0.2 |
GB5009.268 |
|
Cr(Chromium)铬 |
0.3 |
||
|
Pb(Lead)铅 |
0.5 |
||
|
Ni(Nickel)镍 |
0.5 |
||
|
Sb(Antimony)锑 |
2 |
||
|
As(Arsenic)砷 |
0.2 |
||
|
Hg(Mercury)汞 |
0.1 |
电感耦合等离子体质谱仪
对比化学测试项目(GB&FDA&TPD)
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
烟油类 |
Nicotine Consistency |
Anabasine |
X |
√ |
X |
FDA定义了安纳巴松 |
|
Nicotine(a power level,5 data of nicotine) |
√ |
√ |
√ |
|||
|
Carbonyl Compounds |
Formaldehyde |
20 |
√ |
√ |
|
|
|
Acetaldehyde |
20 |
√ |
√ |
|||
|
Acrolein |
16 |
√ |
√ |
|||
|
Crotonaldehyde |
X |
√ |
√ |
|||
|
Diacetyl(2，3-Butadione) |
20 |
√ |
√ |
|||
|
Acetyl Propionyl |
X |
√ |
X |
|||
|
Pentane 2,3 dione |
X |
X |
√ |
|||
|
Heavy Metals |
Cd(Cadmium) |
0.2 |
√ |
√ |
GB管控6种 |
|
|
Cr(Chromium) |
0.3 |
√ |
√ |
|||
|
Pb(Lead) |
0.5 |
√ |
√ |
|||
|
Ni(Nickel) |
0.5 |
√ |
√ |
|||
|
Sb(Antimony) |
X |
X |
√ |
|||
|
As(Arsenic) |
0.2 |
X |
√ |
|||
|
Fe(Iron) |
X |
X |
√ |
|||
|
Al(Aluminum) |
X |
X |
√ |
|||
|
Sn(Tin) |
X |
X |
√ |
|||
|
Hg(Mercury) |
0.1 |
X |
√ |
|||
|
Cu(Copper) |
X |
X |
√ |
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
烟油类 |
Ammonia |
Ammonia |
X |
√ |
X |
FDA |
|
Aromatic Amines |
4-Aminobiphenyl |
X |
√ |
X |
FDA |
|
|
1-Aminonaphthalene |
X |
√ |
X |
|||
|
2-minonaphthalene |
X |
√ |
X |
|||
|
Polyartomatic Hydrocarbon |
Benzo(a)pyrene |
X |
√ |
X |
FDA |
|
|
Glycol |
Menthol |
X |
√ |
X |
FDA提到薄荷醇 |
|
|
Methanol |
√ |
X |
X |
|||
|
Ethylene Glycol |
√ |
√ |
√ |
|||
|
Diethylene Glycol |
√ |
√ |
√ |
|||
|
Tobacco-Specific Nittrosamines |
4-(N-methylnitrosamino)-1-(3-pyridyl)-1-butanone(NNK) |
√ |
√ |
√ |
GB提到NAB+NAT |
|
|
N-nitrosonornicotine(NNN) |
√ |
√ |
√ |
|||
|
N-亚硝基假本贼碱(NAB) |
√ |
X |
X |
|||
|
N-亚硝基新烟碱 |
√ |
X |
X |
|||
|
Volatile |
Acrylonitrile |
X |
√ |
X |
FDA提到丙烯腈 |
|
|
Benzene |
√ |
√ |
√ |
|||
|
1,3-Butadiene |
X |
√ |
√ |
|||
|
Isoprene |
X |
√ |
√ |
|||
|
Toluene |
√ |
√ |
√ |
|||
|
乙苯 |
√ |
X |
X |
|||
|
二甲苯(含对二甲苯,间二甲苯邻二甲苯) |
√ |
X |
X |
|||
|
邻苯二甲酸酯类 |
17种邻苯二甲酸酯类物质总量 |
√ |
X |
X |
GB |
|
Type |
Category |
Test Items |
GB |
FDA |
TPD |
Remark |
|
释放物类 |
气溶胶释放稳定性 |
气溶胶释放稳定性 |
25% |
X |
X |
GB |
|
烟碱释放稳定性 |
Nicotine |
25% |
√ |
√ |
GB提到偏差量 |
|
|
Carbonyl Compounds |
Formaldehyde |
200 |
X |
200 |
GB管控4项 |
|
|
Acetaldehyde |
3200 |
X |
3200 |
|||
|
Acrolein |
16 |
X |
16 |
|||
|
Crotonaldehyde |
X |
X |
√ |
|||
|
Diacetyl(2，3-Butadione) |
140 |
X |
X |
|||
|
Heavy Metals |
Cd(Cadmium) |
0.2 |
√ |
2 |
GB管控7项 |
|
|
Cr(Chromium) |
0.3 |
√ |
3 |
|||
|
Pb(Lead) |
0.5 |
√ |
5 |
|||
|
Ni(Nickel) |
0.5 |
√ |
5 |
|||
|
Sb(Antimony) |
2 |
X |
20 |
|||
|
As(Arsenic) |
0.2 |
X |
√ |
|||
|
Fe(Iron) |
X |
X |
√ |
|||
|
Al(Aluminum) |
X |
X |
√ |
|||
|
Sn(Tin) |
X |
X |
√ |
|||
|
Hg(Mercury) |
0.1 |
X |
√ |
|||
|
Cu(Copper) |
X |
X |
√ |
|||
|
Ammonia |
Ammonia |
X |
√ |
X |
FDA |
|
|
Humectants |
Ethylene Glycol |
X |
√ |
X |
FDA |
|
|
Diethylene Glycol |
X |
√ |
X |
|||
|
Glycerol |
X |
√ |
X |
|||
|
Propylene Glycol |
X |
√ |
X |
|||
|
Nitrosamines,TSNA |
NNK |
X |
√ |
X |
FDA |
|
|
NNN |
X |
√ |
X |